Organic Chemistry I Lab

Course outline

DATE  EXPERIMENT   WILLIAMSON REF.  TOPIC

Tu 6/6/00 1 Ch1; Ch2; Ch9, expt 1 Check in, safety, thin layer chromatography (TLC)

Th 6/8/00 2 Ch 4, expts 2 and 4 Melting point of pure urea and an unknown

Tu 6/13/00 3 Ch 3, expts 1, 2 Solubility tests, recrystallization

Th 6/15/00 4 Ch 18, expt 1 Radical halogenation of 1-chlorobutane

Tu 6/20/00 5 Ch 8, expt 1 (modified) Separation of benzoic acid from benzophenone

Th 6/22/00 6 Ch 5, expts 2, 3 (modified) Simple and fractional distillation
We will be separating hexane from methylcyclohexane

Tu 6/27/00 7 Ch 16, expt 1 Preparation of 1-bromobutane

Th 6/29/00 8 Ch 11, expt 1 (modified) Dehydration of 2-methyl-2-pentanol

Tu 7/4/00 9 Ch 62, expts 1 (2nd half), 4     Synthesis of luminol, chemiluminescence

Th 7/6/00 - - Exam

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